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You are here: Home / Archives for NMR

Conjugated Diolefins Analysis by COSY NMR

January 28, 2008 by process nmr Chemistry, NMR

Conjugated diolefins are responsible for fouling of many processes in a refinery. COSY NMR analysis can determine the concentration of these species in many processed petroleum product streams….see PNA webs site.

Conjugated Olefins by COSY NMR - 1D 1H NMR - Coker Naphtha

Conjugated Olefins by COSY NMR - COSY - Coker Naphtha Showing Conjugated Olefin Signals

Conjugated Olefins by COSY NMR - Hydrotreated Naphtha

Conjugated Olefins by COSY NMR - Hydrotreated Naphtha

Schering-Plough Corporation Seeks Process Analytical Technology Manager

October 29, 2007 by process nmr IR-ATR, NIR, NMR, PAT, Process NMR

Title:
Process Analytical Technology (PAT) Manager

Description:
Implement Process Analytical Technology (PAT) throughout all the Global Quality Sites to identification of incoming materials and monitor manufacturing processes.
Work directly with the sites and Schering Plough Research Institute to help support / initiate the development, validation, and deployment of PAT at the sites.
Review, evaluate, implement, and manage PAT activities.
Provide guidance / technical help to the sites to conduct evaluation and purchase commercial PAT related analytical equipment (e.g. NIR / FT-NIR, Raman / FT-Raman, IR / FT – IR etc.).
Maintain analytical instruments in the lab to comply with cGMP standards and requirements.
Train and mentor laboratory staff on PAT to generate analytical data for routine experiments.
Generate network and infrastructures with various sites of the corporation.
Take full ownership / responsibility and provide effective, meaningful, result driven and pro-active leadership on all PAT projects.
Responsible to transfer knowledge / technology of PAT related projects and activities to sites. Job is located in New Jersey.

Respectfully, Vincent L. Graziano
Recruiting Manager / Global Staffing
Schering-Plough Corporation
556 Morris Avenue, S1-1
Summit, N.J. 07901
Ph: 908-473-2745
Fx: 908-473-2793
Ph: 908-298-5232 (Kenilworth)
Careers: Employment Opportunities
email: vincent.graziano@spcorp.com 

NPS – IS : A New Approach to Process Analytical

October 29, 2007 by process nmr Chemistry, Energy, IR-ATR, NIR, NMR, Process NMR, TD-NMR

Press Release – NMR Process Systems – Swagelok Technology Conference, Teaneck NJ – October 23, 2007

NMR Process Systems, LLC Announces :

Process NMR Associates Develops Oxford QP-20 Spectrometer Replacement

October 29, 2007 by process nmr NMR, Process NMR

In a joint development effort Process NMR Associates and Resonance Systems Ltd have developed a replacement NMR spectrometer for the Oxford QP-20 TD-NMR analyzer. In many cases the excellent magnet and probe of the QP-20 continue to work effectively long after the NMR spectrometer has died. The Spin Track-20 spectrometer enables the user to completely replace the QP-20 NMR system while retaining the use of the original magnet and probe configuration. The product represents state-of-the-art digital NMR technology allowing newly developed TD-NMR methodologies to be applied to complex systems with all the advantages of a windows computer system (replacing the paper cartridge of the original system). Customers who have malfunctioning QP-20 NMR systems can obtain a modern digital NMR system within 8 weeks of order and for less than $16,000. The modular design of the Spin Track TD-NMR systems allows our engineers to develop replacement systems for all benchtop NMR systems such as those marketed by Oxford Instruments, Bruker Minispec, and Resonance Systems. Contact us if you have a non-functioning system that might be a candidate for the Spin Track upgrade.

For more information contact John Edwards Principal, Process NMR Associates – Spin Track Division
87A Sand Pit Rd, Danbury, CT 06810 U.S.A. Tel: (203) 744-5905

PNA Presentation at 9th Upstate NY NMR Symposium

October 7, 2007 by process nmr NMR, Process NMR

State University of New York
College of Environmental Science and Forestry (SUNY-ESF)
Syracuse, NY, 13210
Alumni Lounge– Marshall Hall
October 12, 2007

Co-Organizers

SUNY-ESF Syracuse University SUNY Upstate Medical University Bristol-Myers Squibb
Art Stipanovic Phil Borer Stewart Loh Doug Weaver
Dave Kiemle Stephan Wilkens  

Sponsors

  • SUNY-ESF
  • Syracuse University
  • Bruker Biospin
  • Bristol-Myers Squibb
  • Process NMR Associates LLC
  • Isotec
  • Cambridge Isotope Laboratories
  • Varian Inc.

The 9th annual Upstate NY NMR Symposium will be held at SUNY-ESF on Friday, October 12th featuring keynote speaker Professor Ruth E. Stark, Director Institute for Macromolecular Assemblies, CUNY. Others from around the region will also highlight their work in short presentations and posters.

  • Tentative oral presentation program
  • Poster session program (posted by 9/12)

There is no cost to attend this symposium due to the generosity of the sponsors listed above but pre-registration is required

  • Registration form

Lodging arrangements have not been made for this symposium but a variety of options are available:

  • Lodging Options

The conference will be held in the Alumni Lounge (a.k.a. Nifkin Lounge), Marshall Hall on the SUNY-ESF campus located adjacent to Syracuse University.

  • Maps and Directions

Parking has been arranged in the Irving Garage just a short walk from Marshall Hall (campus map).

Tentative Program

Time Place Speaker Title
8:00-9:10 AM Alumni Lounge
Marshall Hall
Check-In
Coffee + Bagels
Poster Setup
Posters on Display
9:15 Alumni Lounge Phil Borer
Syracuse University
Welcome
9:30 “ Thomas Szyperski
SUNY-Buffalo
Where do we stand on GFT projection NMR spectroscopy?
9:55 “ Yibing Wu
SUNY-Buffalo
GFT-NMR based high throughput structure determination exemplified for NESG targets NeT4 and SR500A
10:10 “ Arindam Ghosh
SUNY-Buffalo
NMR structure of NESG target MR32, a member of the family of Trm112p-like proteins
10:25 “ Bio-Break
10:35 “ David LeMaster Wadsworth Center – NYS Dept. of Health Electrostatic stabilization and general base catalysis in the active site of the human protein disulfide isomerasea domain monitored by hydrogen exchange
11:00 “ Joseph Hornack
RIT
The relaxivity of Gd-(DTPA-BMA) / Cu+2 mixtures and evidence for a Gd-(DTPA-BMA)-Cu complex.
11:25 “ Nelly Aranibar
Bristol-Myers Squibb
Metabolomics in Drug Discovery and development
11:50 “ Lunch
Poster Session
 
1:30 PM 140 Baker Lab Nikolaos Sgourakis
Rensselaer Polytechnic Institute
Pressure Effects on the Ensemble Dynamics of ubiquitin at the Picosecond-to-Nanosecond timescale investigated with isotropic reorientational eigenmode dynamics
1:55 “ Paul Giammatteo or John Edwards
Process NMR Associates, LLC
New Developments in Non-traditional NMR Applications
2:25 “ George Crull
Bristol-Myers Squibb
Extending Solid State NMR to Address Process Development Issues
2:50 “ Gwen Lubey
P+G Pharmaceuticals
Solid State NMR Characterization of Risedronate Hydrate Forms and Dehydrated Risedronate
3:15 “ – Break
3:30 Keynote Lecture Prof. Ruth Stark
CUNY
NMR Structural Studies of Protective Plant Biopolymers
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