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Industrial NMR Spectroscopy Applications

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Test Methods Preformed

Official NMR Methods Performed by Process NMR Associates

D3701-01:  Standard Test Method for Hydrogen Content of Aviation Turbine Fuels by Low Resolution Nuclear Magnetic Resonance Spectrometry – Has been replaced by D7171-05 below

D4808-01:  Standard Test Methods for Hydrogen Content of Light Distillates, Middle Distillates, Gas Oils, and Residua by Low-Resolution Nuclear Magnetic Resonance Spectroscopy – Has been replaced by D7171-05 below

D7171-05: Standard Test Method for Hydrogen Content of Middle Distillate Petroleum Products by Low-Resolution Pulsed Nuclear Magnetic Resonance Spectroscopy – Overview Presentation

D4273-05: Standard Test Methods for Polyurethane Raw Materials Determination of Primary Hydroxyl Content of Polyether Polyols  –  Overview Article

D4875-05:  Standard Test Methods of Polyurethane Raw Materials: Determination of the Polymerized Ethylene Oxide Content of Polyether Polyols – Overview Article

D5017-96: Standard Test Method for Determination of Linear Low Density Polyethylene (LLDPE) Composition by Carbon-13 Nuclear Magnetic Resonance

D5292-99: Standard Test Method for Aromatic Carbon Contents of Hydrocarbon Oils by High Resolution Nuclear Magnetic Resonance Spectroscopy – Overview Article

F2259-03: Standard Test Method for Determining the Chemical Composition and Sequence in Alginate by Proton Nuclear Magnetic Resonance (1H NMR) Spectroscopy – Overview Article

F2260-03: Standard Test Method for Determining Degree of Deacetylation in Chitosan Salts by Proton Nuclear Magnetic Resonance (1H NMR) Spectroscopy

ASTM – Simulated Distillation by Gas Chromatography

D2887: Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography

D3710: Standard Test Method for Boiling Range Distribution of Gasoline and Gasoline Fractions by Gas Chromatography

D5307: Standard Test Method for Determination of Boiling Range Distribution of Crude Petroleum by Gas Chromatography

D6352: Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700°C by Gas Chromatography

USP

Poloxamer Testing

USP <761>: Purity Assays for Pharmaceutical Release

UOP

935-94:   Mercaptan Types In Kerosene by NMR

ISO

10565:1998   Oil and Moisture in Seeds by Low Field NMR Spectroscopy

8292     Animal and vegetable fats and oils — Determination of solid fat content — Pulsed nuclear magnetic resonance method

21461:2006  Rubber – Determination of the aromaticity of oil in vulcanized rubber compounds

21561:2005 Styrene-butadiene rubber (SBR) – Determination of the microstructure of solution-polymerized SBR

11543:2000  Modified starch — Determination of hydroxypropyl content — Method using proton nuclear magnetic resonance (NMR) spectrometry

10632:2000  Oilseed residues — Simultaneous determination of oil and water contents — Method using pulsed nuclear magnetic resonance spectroscopy

AOCS

Cd 16b-93 : (revised in 2000): Direct Method – Determination of Solid Fat Content — Pulsed Nuclear Magnetic Resonance Method

Cd 16-81 : (revised in 2000): Indirect Method – Determination of Solid Fat Content — Pulsed Nuclear Magnetic Resonance Method

Ak5-01 (01) : Oil Content of Oilseed Residues by NMR

Ak3-94 (00) : Oil Content in Rapeseed and other Oilseeds by NMR

Ak4-95 (99):Simultaneous Determination of Oil and Moisture Contents of Oilseeds using Pulsed Nuclear Magnetic Resonance Spectroscopy

European Pharmacopoeia

Salmon Oil, Farmed 01/2005:1910  13C NMR for distribution of fatty acids.

IASC

Aloe Vera – 1H NMR Method for Quality Inspection and Identification – see details.

Canadian Crude Quality Technical Association

Maxxam V1.04 11/05 : Determination of Olefin Content of Crude Oils, Condensates and Diluents by 1H NMR  – see method details

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